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49771
Fluka
Glycerol
puriss. p.a., matrix substance for MALDI-MS, anhydrous, ≥99.0% (GC)
| Synonym: | 1,2,3-Propanetriol, Glycerin |
| CAS Number: | 56-81-5 |
| Linear Formula: | HOCH2CH(OH)CH2OH |
| Molecular Weight: | 92.09 |
| Beilstein Registry Number: | 635685 |
| EC Number: | 200-289-5 |
| MDL number: | MFCD00004722 |
| PubChem Substance ID: | 24873138 |
Description
| Application | Forms a liquid composite matrix with 4-HCCA and 3-aminoquinoline for analysis of neutral and acidic glycans. Glycerol has also been used as a matrix for fast atom bombardment MS.1,2 |
| Glycerol is used both in sample preparation and gel formation for polyacrylamide gel electrophoresis. Glycerol (5-10%) increases the density of a sample so that the sample will layer at the bottom of a gel’s sample well. Glycerol is also used to aid in casting gradient gels and as a protein stabilizer and storage buffer component. |
Properties
| grade | matrix substance for MALDI-MS |
| vapor density | 3.1 (vs air) |
| vapor pressure | <1 mmHg ( 20 °C) |
| puriss. p.a. | |
| assay | ≥99.0% (GC) |
| autoignition temp. | 698 °F |
| refractive index | n |
| bp | 182 °C/20 mmHg(lit.) |
| mp | 20 °C(lit.) |
| density | 1.25 g/mL(lit.) |
| anion traces | chloride (Cl-): ≤1 mg/kg |
| sulfate (SO42-): ≤10 mg/kg | |
| cation traces | Ba: ≤5 mg/kg |
| Ca: ≤5 mg/kg | |
| Cd: ≤1 mg/kg | |
| Co: ≤1 mg/kg | |
| Cr: ≤1 mg/kg | |
| Cu: ≤1 mg/kg | |
| Fe: ≤1 mg/kg | |
| K: ≤20 mg/kg | |
| Mg: ≤1 mg/kg | |
| Mn: ≤1 mg/kg | |
| NH4+: ≤5 mg/kg | |
| Na: ≤20 mg/kg | |
| Ni: ≤1 mg/kg | |
| Pb: ≤1 mg/kg | |
| Zn: ≤1 mg/kg | |
| suitability | in accordance for UV test |
Safety
| Personal Protective Equipment | Eyeshields, Gloves, half-mask respirator (EU), half-mask respirator (US), multi-purpose combination respirator cartridge (US) |
| WGK Germany | 1 |
| RTECS | MA8050000 |
| LEL | 0.90%(V) |
| Flash Point(F) | 320 °F |
| Flash Point(C) | 160 °C |
References
| Cited Reference | 1. Dreisewert, K., et al., , Analysis of native milk oligosaccharides directly from thin-layer chromatography plates by matrix-assisted laser desorption/ionization orthogonal-time-of-flight mass spectrometry with a glycerol matrix. J. Am. Soc. Mass Spectrom. 17, 139-50, (2006) Abstract |
| 2. Suzuki, S., et al., , Comparison of the sensitivities of various derivatives of oligosaccharides in LC/MS with fast atom bombardment and electrospray ionization interfaces. Anal. Chem. 68, 2073-83, (1996) Abstract | |
| reference | , Andrews, A.T. Electrophoresis: Theory, Techniques, and Biochemical and Clinical Applications 2nd ed., New York , (1988), 252 |
| , Link, A.J. ed., 2-D Proteome Analysis Protocols. Methods Mol. Biol. Totowa, NJ , (1999) 112 | |
| Merck | Merck 13,4497 |
| Beilstein | Beil. 1,IV,2751 |
| Aldrich MSDS 1, 993:A / Corp MSDS 1 (1), 1782:D / FT-IR 2 (1), 265:B / FT-IR 1 (1), 183:A / FT-NMR 1 (1), 283:C / IR-Spectra (2), 103:G / IR-Spectra (3), 112:A / NMR-Reference 2 (1), 171:B / RegBook 1 (1), 185:A / Sax 6, 1479 / Sigma FT-IR 1 (1), 1340:B / Structure Index 1, 24:C:7 / Vapor Phase 3, 262:A |
